Download Inorganic Syntheses, Vol. 19 by Duward F. Shriver PDF

By Duward F. Shriver

The volumes during this carrying on with sequence offer a compilation of present recommendations and concepts in inorganic artificial chemistry. contains inorganic polymer syntheses and education of vital inorganic solids, syntheses utilized in the improvement of pharmacologically energetic inorganic compounds, small-molecule coordination complexes, and similar compounds. additionally includes important info on transition organometallic compounds together with species with metal-metal cluster molecules. All syntheses awarded right here were demonstrated.

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6. 7. 8. 9. I. F. Shchegolev,Phys. Status Soiidi (B), 12,9 (1972). A. F. Garito and A. J. Heeger, Acc. , 7, 218 (1974). Z. Soos, Ann. Rev. Phys. Chem, 25, 121 (1974). A. N. Block, in Charge and Energy Transfer in Organic Semiconductors, K. Masuda and M. ), Plenum Press, New York, 1974. D. S. Acker and W. R. Hertler,J. Am. Chem. 84, 3370 (1962). F. Wudl, G . M. Smith, and E. J. , 1970, 1453. D. L. , 1970, 2633. D. L. Coffen, J. Q. Chambers, D. R. Williams,P. E. Garrett, and N. D. Chambers, J. Am.

5HzO] ,IT4 although they have quite different degrees of partial oxidation. Both compounds are of considerable interest as candidates for detailed physical studies, provided that methods for growing single crystals of high quality can be developed. H20 with CO (1 atm) at 150°C, but they formulated the compound as Ir(C0)3C1. The preparation given below is due to Fischer and Brenner,6 who also assigned the integral stoichiometry. The method for prepar*Bell Laboratories, Murray Hill, NJ 07974. Chemistry Division, Argonne National Laboratory, Argonne, IL 60439.

H. Kravitz, and S. Kirschner, P. Ostrowski, and P. Nigray, J. Chem. Educ.. 55, 181 (1978). 11. J. Fujita, A. E. Martell, and K. Nakamura, J. Chem. , 36, 324,331 (1962). 5. LINEAR-CHAIN IRIDIUM CARBONYL HALIDES Submitted by A. P. C,* J. W. KOEPKE,* and C. R. SPRINKLE* Checked by VICKIE HACLEYt and A. H. REIS, JR.? 601r(C0)2C12. 5H20 stacks of planar c i ~ - [ 1 r ( C O ) , C l ~ ] ~units . 5HzO] ,IT4 although they have quite different degrees of partial oxidation. Both compounds are of considerable interest as candidates for detailed physical studies, provided that methods for growing single crystals of high quality can be developed.

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