Download High Pressure Chemistry: Proceedings of the NATO Advanced by Peter L. M. Heydemann (auth.), H. Kelm (eds.) PDF

By Peter L. M. Heydemann (auth.), H. Kelm (eds.)

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Read Online or Download High Pressure Chemistry: Proceedings of the NATO Advanced Study Institute held in Corfu, Greece, September 24 – October 8, 1977 PDF

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Additional resources for High Pressure Chemistry: Proceedings of the NATO Advanced Study Institute held in Corfu, Greece, September 24 – October 8, 1977

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25 GENERATION AND MEASUREMENT OF PRESSURE The ion-like repulsion terms are only a small part of the total repulsion. It is therefore possible to reduce the number of constants by relating the constants in the ion-like repulsion terms to band p, and further expressing pt/p and p_/p in terms of the ionic radii, and b+/b and b_/b in terms 0 the polarizabilities. To determine the parameters p, b and A equ. (27) is evaluated for T ,p and r . The equation is then multipled with V, differentiated with ~espgct to ~, and evaluated again at p.

45 GENERATION AND MEASliREME NT OF PRESSURE Fig. 29 Photograph of 4-wire feedthrough for 700 MPa. with silicone oil and varnish. sheothed wire with one two or four conductors stainless steel cone . 89-- - Fig. 30 Details of a 2 . 5 GPa plug with electrical feedthrough. All dimensions in centimeters. Sealed PETER L. M. 4.. cylinder wire piston Fig. 31 Electrical feed-through for pressures to 3 GPa, DC to 30 MHz. The sheathed wire is silver-soldered into the steel button. 5 mm. GENERATION AND MEASUREMENT OF PRESSURl: 47 the baking process is repeated.

29 shows a photograph of a finished feed-through. 5 GPa is shown in Fig. 30. It is also based on sheathed thermocouple wires. A cone of stainless steel is silver - soldered over the sheathed wire. This cone is seated with a dab of vaseline in a conical set with the same solid angle of 16 to 20 degrees. The conical seat terminates in a straight hole whose diameter is slightly larger than the outside diameter of the sheath. This is an unsupported area seal. 5 GPa the cone can usually be lifted out of the seat with two fingers.

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